For a bit of context I've been trying to get the nmr lab windows cleaned for almost 4 years.

Though Im used to liquids and using Cr(acac)3. What Ga compound do you recommend in solids? And in what concentration?

I was trying to avoid it but it looks like if I want to keep my sanity and get results to collaborators in a decent time frame I may have to.

nope. OOoo where are you headed?

When you run them manually it doens't matter but for some reason ICON likes *needing* the 1d reference. I switched out to au_zg but it then only collected as a 1d (possibly might have messed up the new pulse sequence settings, still jetlagged).

Thanks Clemens!

They are being held onto, just now in the deep dark depths of a basement store room, until our last inova gets decommissioned.