Matthew V. Joannou
@chicagochemo.bsky.social
Inorganic chemist masquerading as a process chemist at Bristol Myers Squibb 💃👨🔬
GC with helium as the carrier gas, GC-MS in single ion mode to detect for water only, IR (but not sure how low the detection limit is). Or, NMR the solvent with a sealed insert of C6D6 and TpyNiMe and see if you see methane. If I could send you a KF...I would, it's the best 🤓 good luck!
March 8, 2025 at 8:13 PM
GC with helium as the carrier gas, GC-MS in single ion mode to detect for water only, IR (but not sure how low the detection limit is). Or, NMR the solvent with a sealed insert of C6D6 and TpyNiMe and see if you see methane. If I could send you a KF...I would, it's the best 🤓 good luck!