1. Maybe SC and powder were measured at different temperatures and the structure is anisotropic.
2. Strong preferred orientation in powder.
3. SQUEEZE was used in SC.
Even so it is up to authors to explain such difference.
Realistically - two difference phases.
1. Maybe SC and powder were measured at different temperatures and the structure is anisotropic.
2. Strong preferred orientation in powder.
3. SQUEEZE was used in SC.
Even so it is up to authors to explain such difference.
Realistically - two difference phases.
www.mindat.org/min-43931.html
www.mindat.org/min-43931.html
For how long, in what range? - to reach decent statistics; where it is still diffracting.
Is there anything specific you do? - Checking calibration and alignment of capillary :)
Software: Fox, TOPAS, Fullprof, EXPO, etc.
For how long, in what range? - to reach decent statistics; where it is still diffracting.
Is there anything specific you do? - Checking calibration and alignment of capillary :)
Software: Fox, TOPAS, Fullprof, EXPO, etc.